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Characterization and Design of Zeolite Catalysts: Solid by Miki Niwa

By Miki Niwa

Zeolites are microporous, aluminosilicate minerals wide-spread as advertisement adsorbents. Zeolite-based catalysts are utilized by business chemical businesses within the interconversion of hydrocarbons and the alkylation of fragrant compounds. the present e-book offers with the characterization of particular homes of Zeolites and calculations for the layout of catalysts. Measurements and usage of strong acidity, form selectivity, and loading houses, which are 3 famous houses of a Zeolite catalyst, are handled intimately. those gains obstacle chemical vapor deposition of silica, form selectivity, loading homes, stable job, Brønsted or Lewis personality, ammonia temperature programmed desorption, keep watch over of the pore-opening measurement through chemical vapor deposition of silica and XAFS research of metals being hugely dispersed in and out a framework.

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Additional resources for Characterization and Design of Zeolite Catalysts: Solid Acidity, Shape Selectivity and Loading Properties

Example text

4. Band position is corrected, and difference spectra are calculated. Absorption band positions are identified from the difference spectra. IR-TPD for each adsorbed species and OH is calculated. Parameters to cancel the difference in extinction coefficients are determined so as to fit the IR-TPD to the MS-TPD. 5. The number and strength of the acid sites are measured. When the distribution is observed, numbers and strengths of acid sites are measured individually. Thus not only the number and the strength are measured, but also the structure of acid site is determined.

Katada, M. Niwa, Catal. Surveys Asia 8, 161 (2004) 11. M. Niwa, N. Katada, J. Jpn. Petrol. Inst. 52, 172 (2009) 12. J. Cvetanovi´c, Y. Amenomiya, Adv. Catal. 17, 103 (1967) 13. L. O. V. H. Lunsford, J. Phys. Chem. 91, 2091 (1987) 14. H. Igi, N. Katada, M. Niwa, in Proceedings of the 12th International Zeolite Conference, vol. 4, ed. J. K. E. B. Higgins (Materials Research Society, Warrendale, 1999), p. 2643 15. W. B. H. L. Schlenker, in Preprint of 11th Discussion on Reference Catalyst (Catalysis Society of Japan, Tokyo, 1987), p.

4. , zeolite species with ca. 100% exchange degree with proton, have been elucidated in previous sections. It is interesting that two to four kinds of acid sites are clearly revealed by utilizing an advantageous property of the IRMS-TPD experiment. In the next step, the distribution of these acid sites is studied with varying the degree of exchange on the NaH-type mordenite and chabazite. The stability of the acid site which depends on the structure or the site location is studied. 5 12-ring 0 0 20 40 60 80 100 1-[Na]/[Al] (ion exchange degree)/ % Fig.

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