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Additional info for Electron Paramagnetic Resonance Volume 23
122 This radical salt is stable indeﬁnitely in the solid but decomposes slowly in DME or THF solutions. 0043(1) consistent with hyperﬁne coupling 40 | Electron Paramag. 163 mT). The small value of the HFS is consistent with a p radical. 3 Tricoordinate phosphine radical cations The use of steric shielding from 2,6-diisopropylphenyl groups is now known to render phosphoniumyl radical cations stable and isolable. 1 mT indicates that the radicals are not entirely planar either in solution or in the solid state.
By contrast, the isomeric 1,4-species 30 shows quinoidal character and is diamagnetic. 107 Disilenes with a Si¼Si double bond are known to readily undergo oxidation or reduction because of their high-lying HOMOs and low-lying LUMOs compared with those of the corresponding alkene analogues, which makes possible the construction of a one-electron reversible redox system. 30 mT) due to coupling of the unpaired electron with the central 29Si nuclei. 80 mT), consistent with delocalization of the unpaired electron over both silicon nuclei in 31.
Yamauchi, J. Am. Chem. , 2010, 132, 9746. 20 | Electron Paramag. , 2013, 23, 1–21 30 Y. Uchida, N. Ikuma, R. Tamura, S. Shimono, Y. Noda, J. Yamauchi, Y. Aoki and H. Nohira, J. Mater. , 2008, 18, 2950–2952. 31 I. Haller, Prog. , 1975, 10, 103. 32 V. Manjuladevi and N. V. Mandhusadana, Curr. , 2003, 85, 1056. 33 Y. Noda, S. Shimono, M. Baba, J. Yamauchi, N. Ikuma and R. Tamura, Appl. Magn. , 2008, 33, 251. 34 K. Suzuki, Y. Uchida, R. Tamura, S. Shimono and J. Yamauchi, J. Mater. , 2012, 22, 6799.